MettlerTrial
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ABCDEFGHIJKLMNOPQRSTUVWXYZAAABACADAEAFAGAHAI
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runadditional solventsolvent amount (ml)furfurylamine (ml)Furfurylamine (mmol)benzaldehyde (ml)Benzaldehyde (mmol)boc-gly (ml)Boc-Gly (mmol)t-butylisonitrile (ml)t-butylisocyanide (mmol)Limiting Reagent (mmol)Mini Block Rxn tube #wt of the tube-b4 (g)wt of the tube-afterWt of the product (g)Wt of product (mg)Yield %commentAmine Vol From .job file (ml)Amine Vol from .jobfile (mmol)Aldehyde Vol From .job file (mL)Aldehyde Vol from.job file (mmol)Acid Vol From .job file
(mL)
Acid Vol from .job file (mmol)Isocyanide Vol From .job file (mL)Isocyanide Vol from .job file (mmol)Limiting ReagentYield % Based on .job file
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1methanol0.20.510.510.510.511A:22.152.1560.00661.35this is supposed to be the positive control!0.510.510.510.5111.35
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2methanol0.20.61.20.510.510.511A:42.1612.22440.06346314.290.61.20.510.510.61.2114.29
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3methanol0.20.510.61.20.510.511A:62.1652.2110.0464610.370.510.61.20.510.51110.37
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4methanol0.20.510.510.61.20.511A:82.15152.20260.05115111.520.510.510.61.20.51111.52
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5methanol0.20.510.510.510.61.21A:102.12252.18190.05945913.390.510.510.510.51113.39
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6methanol0.20.61.20.61.20.510.511A:122.15252.220.06756815.220.61.20.61.20.510.61.2115.22
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7methanol10.250.50.250.50.250.50.250.50.5B:12.1632.18470.0217229.790.250.50.250.50.250.50.250.50.2519.57
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8methanol10.30.60.250.50.250.50.250.50.5B:32.16272.18670.0242410.820.30.60.250.50.250.50.30.60.510.82
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9methanol10.250.50.30.60.250.50.250.50.5B:52.15432.17220.0179188.070.250.50.30.60.250.50.250.50.58.07
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10methanol10.250.50.250.50.30.60.250.50.5B:72.162.17750.0175187.890.250.50.250.50.30.60.250.50.57.89
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11methanol10.250.50.250.50.250.50.30.60.5B:92.1412.15450.0135146.090.250.50.250.50.250.50.250.50.56.09
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12methanol10.30.60.30.60.250.50.250.50.5B:112.14562.15850.0129135.820.30.60.30.60.250.50.30.60.55.82
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13methanol1.60.10.20.10.20.10.20.10.20.2C:22.1512.18250.03153235.510.10.20.10.20.10.20.10.20.235.51
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14methanol1.60.120.240.10.20.10.20.10.20.2C:42.16452.19050.0262629.310.120.240.10.20.10.20.120.240.229.31
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15methanol1.60.10.20.120.240.10.20.10.20.2C:62.16152.18510.02362426.600.10.20.120.240.10.20.10.20.226.60
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16methanol1.60.10.20.10.20.120.240.10.20.2C:82.14152.16410.02262325.480.10.20.10.20.120.240.10.20.225.48
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17methanol1.60.10.20.10.20.10.20.120.240.2C:102.1422.17660.03463539.000.10.20.10.20.10.20.10.20.239.00
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18methanol1.60.120.240.120.240.10.20.10.20.2C:122.162.19390.03393438.220.120.240.120.240.10.20.120.240.238.22
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19ethanol10.250.50.250.50.250.50.250.50.5D:12.16152.19210.03063113.800.250.50.250.50.250.50.250.50.513.80
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20ethanol10.30.60.250.50.250.50.250.50.5D:32.1462.19090.04494520.250.30.60.250.50.250.50.30.60.520.25
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21ethanol10.250.50.30.60.250.50.250.50.5D:52.16852.18220.0137146.180.250.50.30.60.250.50.250.50.56.18
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22ethanol10.250.50.250.50.30.60.250.50.5D:72.1442.18370.03974017.900.250.50.250.50.30.60.250.50.517.90
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23ethanol10.250.50.250.50.250.50.250.50.5D:92.142.1670.0272712.170.250.50.250.50.250.50.250.50.512.17
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24ethanol10.30.60.30.60.250.50.30.60.5D:112.1632.17960.0166177.490.30.60.30.60.250.50.30.60.57.49
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25ethanol1.60.10.20.10.20.10.20.250.50.2E:22.14772.17850.03083134.720.10.20.10.20.10.20.10.20.234.72
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26ethanol1.60.120.240.10.20.10.20.10.20.2E:42.12242.15250.03013033.930.120.240.10.20.10.20.120.240.233.93
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27ethanol1.60.10.20.120.240.10.20.10.20.2E:62.16222.17870.01651718.600.10.20.120.240.10.20.10.20.218.60
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28ethanol1.60.10.20.10.20.120.240.10.20.2E:82.16052.1790.01851920.860.10.20.10.20.120.240.10.20.220.86
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29ethanol1.60.10.20.10.20.10.20.10.20.2E:102.1412.1630.0222224.800.10.20.10.20.10.20.10.20.224.80
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30ethanol1.60.120.240.120.240.10.20.120.240.2E:122.1232.140.0171719.160.120.240.120.240.10.20.120.240.219.16
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31acetonitrile10.250.50.250.50.250.50.10.20.2F:12.152.2150.0656573.27error in red should change this yield0.250.50.250.50.250.50.250.50.529.31
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32acetonitrile10.30.60.250.50.250.50.250.50.5F:32.1662.25720.09129141.120.30.60.250.50.250.50.30.60.541.12
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33acetonitrile10.250.50.30.60.250.50.250.50.5F:52.14472.22120.07657734.500.250.50.30.60.250.50.250.50.534.50
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34acetonitrile10.250.50.250.50.30.60.250.50.5F:72.16552.22850.0636328.410.250.50.250.50.30.60.250.50.528.41
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35acetonitrile10.250.50.250.50.250.50.250.50.5F:92.1582.21110.05315323.940.250.50.250.50.250.50.250.50.523.94
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36acetonitrile10.30.60.30.60.250.50.30.60.5F:112.142.21350.07357333.140.30.60.30.60.250.50.30.60.533.14
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37acetonitrile1.60.10.20.10.20.10.20.250.50.2G:22.1482.20180.05385460.650.10.20.10.20.10.20.10.20.260.65
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38acetonitrile1.60.120.240.10.20.10.20.10.20.2G:42.1462.19390.04794854.000.120.240.10.20.10.20.120.240.254.00
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39acetonitrile1.60.10.20.120.240.10.20.10.20.2G:62.15252.17540.02292325.820.10.20.120.240.10.20.10.20.225.82
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40acetonitrile1.60.10.20.10.20.120.240.10.20.2G:82.1592.20150.04254347.910.10.20.10.20.120.240.10.20.247.91
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41acetonitrile1.60.10.20.10.20.10.20.10.20.2G:102.16552.220.05455561.44error in red should not change yield0.10.20.10.20.10.20.10.20.261.44
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42acetonitrile1.60.120.240.120.240.10.20.120.240.2G:122.16232.190.02772831.230.120.240.120.240.10.20.120.240.231.23
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43THF10.250.50.250.50.250.50.10.20.2H:12.15782.20.04224247.57error in red should change this yield0.250.50.250.50.250.50.250.50.519.03
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44THF10.30.60.250.50.250.50.250.50.5H:32.14882.16760.0188198.480.30.60.250.50.250.50.30.60.58.48
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45THF10.250.50.30.60.250.50.250.50.5H:52.16572.18060.0149156.720.250.50.30.60.250.50.250.50.56.72
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46THF10.250.50.250.50.30.60.250.50.5H:72.15412.17340.0193198.700.250.50.250.50.30.60.250.50.58.70
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47THF10.250.50.250.50.250.50.250.50.5H:92.14752.16550.018188.120.250.50.250.50.250.50.250.50.58.12
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48THF10.30.60.30.60.250.50.30.60.5H:112.16462.18470.0201209.060.30.60.30.60.250.50.30.60.59.06
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Sheet1