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nano@stanfordedX: Physical Vapor DepositionPhysical vapor deposition (PVD) represents a variety of vacuum deposition techniques that can deposit thin films onto substrates. The material used to form the thin film is often called source material in evaporation, or target in sputtering. The name, physical vapor deposition, indicates that no new chemical bonds are formed at the interface, and the film growth is driven by physisorption. The thickness of PVD films usually range from angstroms to microns. During the PVD process, the use of a high vacuum chamber is essential to achieve high film purity. PVD coatings are widely used in semiconductor devices, solar energy, optics and many other industries. Two main types of PVD, evaporation and sputtering, are introduced here.https://courses.edx.org/courses/course-v1:StanfordOnline+ENGRX0001+1T2020/jump_to/block-v1:StanfordOnline+ENGRX0001+1T2020+type@sequential+block@e9ca7776032d4441815fb5f6f3b0e1f3Deposition (Metallization)Intro/Backgroundyesn/aOnline course (edX, Coursera, Canvas)
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nano@stanfordedX: Chemical Vapor Deposition OverviewChemical vapor deposition is another important thin film deposition technique and it is prevalent throughout industries. CVD can be defined as a process in which the vapor phase gases chemically react on the substrate surface to form thin films. Reactant gases are also known as “precursors”. During a CVD process, precursors are pumped into a reaction chamber, and the chamber is heated to a desired temperature to allow precursor gases to bond with the substrate surfaces. The occurrence of the chemical reaction is essential during the CVD film growth. One of the products of the reaction will deposit onto the substrate as a thin film and the by-products are pumped out. Due to the chemical bonding, the adhesion between the film and the substrate is much stronger compared to typical PVD films.https://courses.edx.org/courses/course-v1:StanfordOnline+ENGRX0001+1T2020/courseware/d3fccb4138f64d03a45ef4a77c97c3d1/3173e47dc49747d481f1e6f371f50753/?activate_block_id=block-v1%3AStanfordOnline%2BENGRX0001%2B1T2020%2Btype%40sequential%2Bblock%403173e47dc49747d481f1e6f371f50753Deposition (Metallization)Intro/Backgroundyesn/aOnline course (edX, Coursera, Canvas)
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nano@stanfordedX: Atomic Layer DepositionAtomic Layer Deposition (ALD) is a thin-film deposition technique based on self-limiting surface reactions. Most ALD reactions involve two gas phase chemicals, also known as “precursors”. The precursors react with the substrate surface in a sequential order in the form of non-overlapping pulses. Each cycle should last long enough until all the reactive sites on the surface are consumed. Due to the self-limiting nature of the reactions, ALD is able to grow pinhole-free and conformal thin films. The thickness of the thin films can be controlled by the number of processing cycles, and films at atomic level precision can be achieved. One of the main motivations for ALD is semiconductor devices fabrication. ALD has been used for applications such as high dielectric constant gate oxides in MOSFET, copper diffusion barriers in interconnects, and solid oxide fuel cells.https://courses.edx.org/courses/course-v1:StanfordOnline+ENGRX0001+1T2020/courseware/bab7a355c5fd4988a072fedca82512ee/8c848ef943d04e0d84421f2f4bb16fe6/?activate_block_id=block-v1%3AStanfordOnline%2BENGRX0001%2B1T2020%2Btype%40sequential%2Bblock%408c848ef943d04e0d84421f2f4bb16fe6Deposition (Metallization)Intro/Backgroundyesn/aOnline course (edX, Coursera, Canvas)
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nano@stanfordedX: Introduction to LithographyThis course covers the basic concepts of photolithography, with focus on general information helpful to orient the learner to understand lithography in a lab and/or cleanroom setting. It should be noted that this is not an exhaustive list of processing steps, and each process module is subject to change depending on the specific aims of the project. https://courses.edx.org/courses/course-v1:StanfordOnline+ENGRX0001+1T2020/courseware/fcc7a069f4bd4294b48cba3e7c4429a3/ad9aa5d945fd4d15b4b784cf64817426/?activate_block_id=block-v1%3AStanfordOnline%2BENGRX0001%2B1T2020%2Btype%40sequential%2Bblock%40ad9aa5d945fd4d15b4b784cf64817426Lithography/Photolithography (Resist, Exposure, Develop, Oven/Hotplate)Intro/Backgroundyesn/aOnline course (edX, Coursera, Canvas)
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nano@stanfordedX: Introduction of Transmission Electron Microscopy (TEM)Introduction of Transmission Electron Microscopy (TEM)https://courses.edx.org/courses/course-v1:StanfordOnline+ENGRX0001+1T2020/courseware/060b0c34ca4e407eb7fb4d143ba2b90b/0ded6fa72d5146af8361f696f52908e5/?activate_block_id=block-v1%3AStanfordOnline%2BENGRX0001%2B1T2020%2Btype%40sequential%2Bblock%400ded6fa72d5146af8361f696f52908e5Microscopy / Imaging (SEM, TEM, FIB, optical, AFM)Intro/BackgroundyesTitan TEMOnline course (edX, Coursera, Canvas)
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nano@stanfordedX: Introduction to Scanning Electron MicroscopyScanning electron microscopy (SEM) is imaging technique in which an image can be produced by scanning a probe formed of electrons across the surface of a sample. Compared to conventional light microscopy, electrons have much shorter wavelength, enabling much higher resolution images with much larger depth of focus. In the light microscopy and SEM images below, compare the amount of detail and depth of focus (also known as depth of field). The purpose of this web module is to prepare new users to take the hands-on training to operate the FEI Sirion SEM at SNSF. https://courses.edx.org/courses/course-v1:StanfordOnline+ENGRX0001+1T2020/courseware/060b0c34ca4e407eb7fb4d143ba2b90b/9d8dfed83a6a43eeaab4e0f4ad27d327/?activate_block_id=block-v1%3AStanfordOnline%2BENGRX0001%2B1T2020%2Btype%40sequential%2Bblock%409d8dfed83a6a43eeaab4e0f4ad27d327Microscopy / Imaging (SEM, TEM, FIB, optical, AFM)TrainingyesMagellan SEMOnline course (edX, Coursera, Canvas)
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nano@stanfordedX: Optical Microscopes OverviewGeneral overview of microscopeshttps://courses.edx.org/courses/course-v1:StanfordOnline+ENGRX0001+1T2020/courseware/060b0c34ca4e407eb7fb4d143ba2b90b/e37e6c06de7345bfa7e5b1fb93fa3478/?activate_block_id=block-v1%3AStanfordOnline%2BENGRX0001%2B1T2020%2Btype%40sequential%2Bblock%40e37e6c06de7345bfa7e5b1fb93fa3478Microscopy / Imaging (SEM, TEM, FIB, optical, AFM)Intro/Backgroundyesn/aOnline course (edX, Coursera, Canvas)
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nano@stanfordedX: Keyence VK-X Series 3D Laser Scanning Confocal MicroscopeThe Keyence VK-X Series 3D Laser Scanning Confocal Microscope provides non-contact, nanometer-level profile, roughness, and film thickness data on any material. The lateral resolution of the microscope is 120 nm using the 408 nm violet laser light. The microscope scans the surface using a 16-bit photomultiplier to receive the reflected laser light. The instrument is able to provide highly accurate 3D measurement data over any shape of materials and steep angles (up to 88 degree angle of detection). High-resolution optical images can be acquired with resolutions up to 21.6 million pixels through 3CCD pixel shifting technology. High dynamic range (16-bit resolution color gradation) function automatically recognizes bright and dark areas as well as low contrast areas.https://courses.edx.org/courses/course-v1:StanfordOnline+ENGRX0001+1T2020/courseware/060b0c34ca4e407eb7fb4d143ba2b90b/6d1e30842d3849c6836a8481dab8e2bb/?activate_block_id=block-v1%3AStanfordOnline%2BENGRX0001%2B1T2020%2Btype%40sequential%2Bblock%406d1e30842d3849c6836a8481dab8e2bbMicroscopy / Imaging (SEM, TEM, FIB, optical, AFM)TrainingyesKeyence VK-X Series 3D Laser Scanning Confocal MicroscopeOnline course (edX, Coursera, Canvas)
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Midwest Nanotechnology Infrastructure Corridor (MINIC)Lab TrainingLab Traininghttps://training.umn.edu/courses/19326Soft & Hybrid Materials (DSC, DLS, GPC, BET, TGA)Trainingn/aOnline course (edX, Coursera, Canvas)Unlicensed
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nano@stanfordedX: Introduction to X-ray Photoelectron SpectroscopyX-ray photoelectron spectroscopy (XPS) is a surface-sensitive spectroscopic technique that can give quantitative elemental composition information on a wide variety of samples. The purpose of this web module is to prepare new users to take the hands-on training to operate the PHI v1 XPS at SNSF. This is a high-level primer and not an exhaustive course on XPS; for those interested in diving deeper, many texts exist.https://courses.edx.org/courses/course-v1:StanfordOnline+ENGRX0001+1T2020/courseware/ba13f23503f4456bbbe04f1c81f3b49d/1b5dc95320d1463d812d36af1a729f15/?activate_block_id=block-v1%3AStanfordOnline%2BENGRX0001%2B1T2020%2Btype%40sequential%2Bblock%401b5dc95320d1463d812d36af1a729f15X-Ray (XRD, XPS, XCT)TrainingyesPHI VersaProbe IIIOnline course (edX, Coursera, Canvas)
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Soft and Hybrid Nanotechnology Experimental (SHyNE) ResourceINCA EDS Instructions: S3400, S4800, and QUANTAhttp://www.nuance.northwestern.edu/docs/epic-pdf/INCA%20EDS%20Operation%20Instructions.pdfChemical / Composition Analysis (Raman, FTIR, UV/Vis, EDS, EBSD)Surface AnalysisTrainingIncaPDF / Word Doc
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Soft and Hybrid Nanotechnology Experimental (SHyNE) ResourceEDS With AZtechttp://www.nuance.northwestern.edu/docs/epic-pdf/2020_user-manuals/eds_aztec_3_2020.pdfChemical / Composition Analysis (Raman, FTIR, UV/Vis, EDS, EBSD)Surface AnalysisTrainingAZtecPDF / Word Doc
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Soft and Hybrid Nanotechnology Experimental (SHyNE) ResourceElectron Backscatter Difraction AZtec - Quanta 650Fhttp://www.nuance.northwestern.edu/docs/epic-pdf/2020_user-manuals/ebsd_3_2020.pdfChemical / Composition Analysis (Raman, FTIR, UV/Vis, EDS, EBSD)TrainingAZtecPDF / Word Doc
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nano@stanford
Lesker2 Sputter TiN Initial Development
Our goal was to develop a process for sputtering of NVM-quality TiN using the new Lesker sputtering tool (Lesker-2) that resides inside the cleanroom. This tool can achieve the high-vacuum pressures necessary for TiN films with low levels of oxygen contamination.
https://snfexfab.stanford.edu/snf/nano-nugget/lesker2-sputter-tin-initial-development
Deposition (Metallization)
Training - more specific information focused on a tool and/or processing or recipes for that tool
TrainingLesker 2PDF / Word Doc
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nano@stanfordSOP for Thin, low temperature ALD of Al2O3 and HfO2 with seed layerTips for deposition of very thin, low temperature Al2O3 in the Savannah in the SNF.https://snfexfab.stanford.edu/snf/nano-nugget/sop-for-thin-low-temperature-ald-of-al2o3-and-hfo2-with-seed-layerDeposition (Metallization)
Training - more specific information focused on a tool and/or processing or recipes for that tool
TrainingSavannahPDF / Word Doc
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nano@stanfordSOP for Seeded ALD deposition on MoS2Standard operating procedures for seed layer aided ALD on 2D materials.https://snfexfab.stanford.edu/snf/nano-nugget/sop-for-seeded-ald-deposition-on-mos2Deposition (Metallization)TrainingAJA evaporatorPDF / Word Doc
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nano@stanfordSOP for Seeded ALD depositions on MOSCAPS and MIMS structures on SiliconProcess to create electrical test structures using metal-seeded ALD layers on silicon substrates. https://snfexfab.stanford.edu/snf/nano-nugget/sop-for-seeded-ald-depositions-on-moscaps-and-mims-structures-on-siliconDeposition (Metallization)TrainingAJA evaporatorPDF / Word Doc
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nano@stanfordNiobium Deposition and Patterning RunsheetProcessing sequence for deposition and patterning of Niobium in the SNF.
https://snfexfab.stanford.edu/snf/nano-nugget/niobium-deposition-and-patterning-runsheet
Deposition (Metallization)Lithography/Photolithography (Resist, Exposure, Develop, Oven/Hotplate)TrainingLesker Sputter, Plasma Therm Versaline LL ICP Dielectric Etcher, Plasma Therm Versaline LL ICP Metal Etcher (PT-MTL)PDF / Word Doc
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nano@stanfordStandard Operating Procedure for MOCVD aix-ccsThis document describes things you need to check before operating the Stanford MOCVD aix-ccs tool for safety and correct operation.https://snfexfab.stanford.edu/snf/nano-nugget/standard-operating-procedure-for-mocvd-aix-ccsDeposition (Metallization)TrainingAix-ccs PDF / Word Doc
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Soft and Hybrid Nanotechnology Experimental (SHyNE) ResourceE-beam Evaporator – AJAAJA E-beam evaporator is for metal deposition on silicon wafers or other compatible substrates.https://cpb-us-e1.wpmucdn.com/sites.northwestern.edu/dist/f/666/files/2015/10/E-beam_Evaporator_AJA-17wwc8c.pdfDeposition (Metallization)TrainingAJA evaporatorPDF / Word Doc
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Soft and Hybrid Nanotechnology Experimental (SHyNE) ResourceSputter I – AJA Orion Sputterhttps://cpb-us-e1.wpmucdn.com/sites.northwestern.edu/dist/f/666/files/2015/10/Sputter-I-AJA-Orion-Sputter_2-20-19-u909bv.pdfDeposition (Metallization)TrainingAJA Orion SputterPDF / Word Doc
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Soft and Hybrid Nanotechnology Experimental (SHyNE) ResourceSputter II – AJA Orion Sputterhttps://cpb-us-e1.wpmucdn.com/sites.northwestern.edu/dist/f/666/files/2015/10/sputter-II-2-20-19-1aw7hnb.pdfDeposition (Metallization)TrainingAJA Orion SputterPDF / Word Doc
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Soft and Hybrid Nanotechnology Experimental (SHyNE) ResourceThermal Evaporator – Denton Vacuum Explorer 14https://cpb-us-e1.wpmucdn.com/sites.northwestern.edu/dist/f/666/files/2015/10/Thermal_Evaporator_Denton_Vacuum_Explorer14-rflz6g.pdfDeposition (Metallization)TrainingDenton Vacuum Explorer 14PDF / Word Doc
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Soft and Hybrid Nanotechnology Experimental (SHyNE) ResourceKJLC Nano38 Thermal Evaporatorhttp://www.nuance.northwestern.edu/docs/epic-pdf/2020_user-manuals/leskermanual_9_2019.pdfDeposition (Metallization)TrainingKJLC Nano38PDF / Word Doc
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Soft and Hybrid Nanotechnology Experimental (SHyNE) ResourceAtomic Layer Deposition – Arradiance GEMStar XT-PThe Arradiance ALD XT-P is full-featured ALD system capable of depositing a wide range of materials conformally over flat and patterned substrates and micro-particles (powders). Both metals and dielectrics can be deposited and multi-material coatings can be produced as well. https://cpb-us-e1.wpmucdn.com/sites.northwestern.edu/dist/f/666/files/2018/06/ALD_GEMStar-06072018-21e1bql.pdfDeposition (Metallization)TrainingArradiance GEMStar XT-PPDF / Word Doc
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Soft and Hybrid Nanotechnology Experimental (SHyNE) ResourceParylene Deposition System – SCS PDS 2010 LABCOTER2It is a vacuum deposition system. Parylene is deposited at about 35 mT from the vapor phase and hence the coating is conformal. Samples of any shape or form get coated all around. https://cpb-us-e1.wpmucdn.com/sites.northwestern.edu/dist/f/666/files/2015/10/SCS-PDS-2010-LABCOTER2-Parylene-Deposition-System-2-19-19-uhpd31.pdfDeposition (Metallization)TrainingSCS PDS 2010 LABCOTER2PDF / Word Doc
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Soft and Hybrid Nanotechnology Experimental (SHyNE) ResourcePlasma Enhanced Chemical Vapor Deposition (PECVD) – STS LpX CVDhttps://cpb-us-e1.wpmucdn.com/sites.northwestern.edu/dist/f/666/files/2015/10/PECVD_STS_LpX_CVD_10212015-1ngr410.pdfDeposition (Metallization)TrainingSTS LpX CVDPDF / Word Doc
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Soft and Hybrid Nanotechnology Experimental (SHyNE) ResourceRapid Thermal Processor – AW-610https://cpb-us-e1.wpmucdn.com/sites.northwestern.edu/dist/f/666/files/2015/10/Thermal_Processor_AW-610_Rapid_Thermal-Processor_Allwin21Corp-18331j1.pdfDeposition (Metallization)TrainingAW-610PDF / Word Doc
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nano@stanford
SOP- Fabrication of an Etched Silicon Platform with Applications in Uniform Dissection of Biological Samples
This document contains standard operating procedures (SOPs) for the following processes: 1.Fabrication of oxide hard mask for deep silicon etching. 2.Tapered etch method for blade formation using ​PT-DSE 3.Through-hole etching using ​PT-DSE
https://snfexfab.stanford.edu/snf/nano-nugget/sop-fabrication-of-etched-silicon-platform-with-applications-in-uniform-dissection-of-biological
Etching (Wet & Dry)
Training - more specific information focused on a tool and/or processing or recipes for that tool
Training
PlasmaTherm CCP-DEP PECVD, Heidelberg, PT-DSE
PDF / Word Doc
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nano@stanfordSOP for Metal Assisted Chemical Etching (MACE)Procedures for doing MACE etching to make tall pillars in silicon.https://snfexfab.stanford.edu/snf/nano-nugget/sop-for-metal-assisted-chemical-etching-maceEtching (Wet & Dry)TrainingAJA evaporatorPDF / Word Doc
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nano@stanfordSOP for Making Vertical Nanostructures with Various ShapesA two stage etching procedure can be used to fabricate various vertical nanostructures for bio-relatedexperiments.https://snfexfab.stanford.edu/snf/nano-nugget/sop-for-making-vertical-nanostructures-with-various-shapesEtching (Wet & Dry)TrainingHeidelberg MLA 150, Plasma Therm Versaline LL ICP Dielectric EtcherPDF / Word Doc
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nano@stanfordSOP- Silicon Oxide Hardmask for Si Etching in PT-DSEStep-by-step procedures and processing tips for fabrication of an SiOx hardmask for deep silicon etch in the SNF.https://snfexfab.stanford.edu/snf/nano-nugget/sop-silicon-oxide-hardmask-for-si-etching-in-pt-dseEtching (Wet & Dry)TrainingPlasmaTherm Shuttlelock PECVD System, Plasma Therm Versaline LL ICP Deep Silicon EtcherPDF / Word Doc
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nano@stanfordStandard Operating Procedures for TMD exfoliation, etching, and transferThe standard operating procedures for 1. Optimal TMD exfoliation on SiO2 substrate, 2. Etching of TMD flakes, 3. Transfer from TMD flakes from SiO2 substrate to a metallic substrate are explained in details.
https://snfexfab.stanford.edu/snf/nano-nugget/standard-operating-procedures-for-tmd-exfoliation-etching-and-transfer
Etching (Wet & Dry)TrainingPDF / Word Doc
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nano@stanfordAddressing Grassing and Overetch in SiO2 HardmaskTroubleshooting tips for roughened surfaces after etch (also called grassing or line edge roughness).https://snfexfab.stanford.edu/snf/nano-nugget/addressing-grassing-and-overetch-in-sio2-hardmaskEtching (Wet & Dry)TrainingOxford III-V etcher, Oxford Dielectric EtcherPDF / Word Doc
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Soft and Hybrid Nanotechnology Experimental (SHyNE) ResourcePlasma Cleaner – Samco PC-300Samco PC300 plasma cleaner has a parallel-plate configuration that can be used in both plasma etching (PE) mode as well as reactive ion etching (RIE) mode for isotropic and anisotropic etching respectively. It can be used for stripping photoresist, descumming, ashing, and surface cleaning or modification for substrate and wire bonding applications.https://cpb-us-e1.wpmucdn.com/sites.northwestern.edu/dist/f/666/files/2018/11/Samco_Plasma_Cleaner_SOP-2of0sse.pdfEtching (Wet & Dry)TrainingSamco PC-300PDF / Word Doc
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Soft and Hybrid Nanotechnology Experimental (SHyNE) ResourceDeep Reactive Ion Etcher (DRIE) – STS LpX PegasusSTS LpX Pegasus is used for deep reactive ion etching of siliconhttps://cpb-us-e1.wpmucdn.com/sites.northwestern.edu/dist/f/666/files/2015/10/DRIE_STS_LpX_Pegasus-u6mdjg.pdfEtching (Wet & Dry)TrainingDeep Reactive Ion Etcher (DRIE) – STS LpX PegasusPDF / Word Doc
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Soft and Hybrid Nanotechnology Experimental (SHyNE) ResourceReactive Ion Etcher (RIE) – Samco RIE-10NRhttps://cpb-us-e1.wpmucdn.com/sites.northwestern.edu/dist/f/666/files/2015/10/Reactive_Ion_EtcherRIE_SamcoRIE-10NR_0-oiq93i.pdfEtching (Wet & Dry)TrainingSamco RIE-10NRPDF / Word Doc
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Soft and Hybrid Nanotechnology Experimental (SHyNE) ResourceXenon Difluoride Etcher – Xactixhttps://cpb-us-e1.wpmucdn.com/sites.northwestern.edu/dist/f/666/files/2015/10/Xenon_Difluoride_Etcher_Xactix-1okys7e.pdfEtching (Wet & Dry)TrainingXactixPDF / Word Doc
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nano@stanford
Self-Assembly Schemes for the Fabrication of Inverse Opals
The nanoscribe can be used to create template structures for particle self assembly, and details about inverse opal BCC and FCC structures are described.
https://snfexfab.stanford.edu/snf/nano-nugget/self-assembly-schemes-for-fabrication-of-inverse-opals
Lithography/Photolithography (Resist, Exposure, Develop, Oven/Hotplate)
Training - more specific information focused on a tool and/or processing or recipes for that tool
TrainingNanoscribePDF / Word Doc
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nano@stanfordImproving adhesion and preventing collapsing of Nanoscribe resist IP-DipAn improved substrate pretreatment protocol is therefore developed that results in better adhesion.https://snfexfab.stanford.edu/snf/nano-nugget/improving-adhesion-and-preventing-collapsing-of-nanoscribe-resist-ip-dipLithography/Photolithography (Resist, Exposure, Develop, Oven/Hotplate)
Training - more specific information focused on a tool and/or processing or recipes for that tool
TrainingPDF / Word Doc
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nano@stanfordSOP for Bioprinting on NanostructuresA guide to using a new PLPP gel protocol developed by Alveolehttps://snfexfab.stanford.edu/snf/nano-nugget/sop-for-bioprinting-on-nanostructuresLithography/Photolithography (Resist, Exposure, Develop, Oven/Hotplate)Lithography/Photolithography (Resist, Exposure, Develop, Oven/Hotplate)
Training - more specific information focused on a tool and/or processing or recipes for that tool
TrainingPrimo AlveolePDF / Word Doc
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nano@stanfordSOP for patterning Si wafers on heidelberg2Some processing details for printing patterns for silicon nanowire fabrication.https://snfexfab.stanford.edu/snf/nano-nugget/sop-for-patterning-si-wafers-on-heidelberg2Lithography/Photolithography (Resist, Exposure, Develop, Oven/Hotplate)TrainingHeidelbergPDF / Word Doc
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nano@stanfordSOP for Nano Imprint LithographyProcedures for doing NIL in preparation for MACE etching.https://snfexfab.stanford.edu/snf/nano-nugget/sop-for-nano-imprint-lithographyLithography/Photolithography (Resist, Exposure, Develop, Oven/Hotplate)TrainingPDF / Word Doc
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nano@stanfordSOP for positive photoresist on NanoscribeSOP for using SPR-220 and AZ4620 positive photoresists on Nanoscribe using the oil immersion mode.https://snfexfab.stanford.edu/snf/nano-nugget/sop-for-positive-photoresist-on-nanoscribeLithography/Photolithography (Resist, Exposure, Develop, Oven/Hotplate)TrainingNanoscribePDF / Word Doc
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nano@stanfordPatterning SPR220 on Reflective Materials with NanoscribePatterning SPR220 on Reflective Materials with Nanoscribehttps://snfexfab.stanford.edu/snf/nano-nugget/patterning-spr220-on-reflective-materials-with-nanoscribeLithography/Photolithography (Resist, Exposure, Develop, Oven/Hotplate)TrainingNanoscribePDF / Word Doc
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nano@stanfordWaveguide fabrication with the Heidelberg MLA150 Maskless Aligner Run SheetIn order to make the lowest loss waveguides, we need to find a combination of dose/defocus and reflow time/temperature that gives us the best resolution and the lowest line edge roughness and line width roughness.https://snfexfab.stanford.edu/snf/nano-nugget/waveguide-fabrication-with-heidelberg-mla150-maskless-aligner-run-sheetLithography/Photolithography (Resist, Exposure, Develop, Oven/Hotplate)TrainingPDF / Word Doc
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nano@stanfordBlock Copolymer Directed Self-Assembly Standard Operating ProcedureIn this standard operating procedure (SOP), we propose a recipe for DSA with 70:30 PS-b-PMMA.https://snfexfab.stanford.edu/snf/nano-nugget/block-copolymer-directed-self-assembly-standard-operating-procedureLithography/Photolithography (Resist, Exposure, Develop, Oven/Hotplate)TrainingPlasma Therm Versaline LL ICP Metal EtcherPDF / Word Doc
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nano@stanfordSilicon Nitride Nanoscale Stencils for Non-destructive Metal Grating PatterningA process flow is presented to create periodic metallic gratings on the order of 150 nm using a stencil lithography technique.https://snfexfab.stanford.edu/snf/nano-nugget/silicon-nitride-nanoscale-stencils-for-non-destructive-metal-grating-patterningLithography/Photolithography (Resist, Exposure, Develop, Oven/Hotplate)TrainingPDF / Word Doc
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nano@stanfordWaveguide fabrication with the Heidelberg MLA150 Maskless AlignerProcess flow for optical waveguide creation using Heidelberg.https://snfexfab.stanford.edu/snf/nano-nugget/waveguide-fabrication-with-heidelberg-mla150-maskless-alignerLithography/Photolithography (Resist, Exposure, Develop, Oven/Hotplate)TrainingHeidelberg MLA 150PDF / Word Doc
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nano@stanfordBasics of Block Copolymer Directed Self AssemblyBlock copolymer Directed Self Assembly (DSA) is a technique used to create high resolution structures without advanced lithography techniques.
https://snfexfab.stanford.edu/snf/nano-nugget/basics-of-block-copolymer-directed-self-assembly
Lithography/Photolithography (Resist, Exposure, Develop, Oven/Hotplate)TrainingPDF / Word Doc
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nano@stanfordGetting Started with Custom Inks on the VolteraWatch E241 students load and print custom ink with the Voltera.
https://snfexfab.stanford.edu/snf/nano-nugget/getting-started-with-custom-inks-on-voltera
Lithography/Photolithography (Resist, Exposure, Develop, Oven/Hotplate)TrainingVoltera PDF / Word Doc
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nano@stanfordStanford Nanoscribe Operating ProcedureThis is the operating procedue written by our researchers for use of our Nanoscribe.
https://snfexfab.stanford.edu/snf/nano-nugget/stanford-nanoscribe-operating-procedure
Lithography/Photolithography (Resist, Exposure, Develop, Oven/Hotplate)TrainingNanoscribePDF / Word Doc
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nano@stanfordBasics of Block Copolymer Directed Self AssemblyBlock copolymer Directed Self Assembly (DSA) is a technique used to create high resolution structures without advanced lithography techniques.https://snfexfab.stanford.edu/snf/nano-nugget/basics-of-block-copolymer-directed-self-assemblyLithography/Photolithography (Resist, Exposure, Develop, Oven/Hotplate)TrainingPDF / Word Doc
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nano@stanfordHelpful hints for grayscale lithography on the Heidelberg MLA 150When using grayscale lithography on the Heidelberg, there are a few quirks that may slow down your progress. This document provides some warnings and helpful tricks to overcome the common roadblocks.https://snfexfab.stanford.edu/snf/nano-nugget/helpful-hints-for-grayscale-lithography-on-heidelberg-mla-150Lithography/Photolithography (Resist, Exposure, Develop, Oven/Hotplate)TrainingHeidelberg MLA 150PDF / Word Doc
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nano@stanfordA Study of Analytical and Empirical Resist Reflow in the LiteratureA summary of the main findings in the literature regarding resist reflow. https://snfexfab.stanford.edu/snf/nano-nugget/study-of-analytical-and-empirical-resist-reflow-in-literatureLithography/Photolithography (Resist, Exposure, Develop, Oven/Hotplate)TrainingPDF / Word Doc
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Soft and Hybrid Nanotechnology Experimental (SHyNE) ResourceMask Aligner – Karl Suss MABA6Contact photolithography https://cpb-us-e1.wpmucdn.com/sites.northwestern.edu/dist/f/666/files/2015/10/Aligner_SussMABA6_Mask_Aligner-1nf9frw.pdfLithography/Photolithography (Resist, Exposure, Develop, Oven/Hotplate)TrainingKarl Suss MABA6PDF / Word Doc
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Soft and Hybrid Nanotechnology Experimental (SHyNE) ResourceMask Aligner – Karl Suss MJB4Contact photolithography https://cpb-us-e1.wpmucdn.com/sites.northwestern.edu/dist/f/666/files/2015/10/Suss-MJB4-Mask-Aligner-1to5thm.pdfLithography/Photolithography (Resist, Exposure, Develop, Oven/Hotplate)TrainingKarl Suss MJB4PDF / Word Doc
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Soft and Hybrid Nanotechnology Experimental (SHyNE) ResourceMaskless Aligner – Heidelberg MLA150Heidelberg MLA150 Maskless Aligner is a full-scale production level laser writer which can be used toperform lithography directly on wafers as well as to create photomasks.https://cpb-us-e1.wpmucdn.com/sites.northwestern.edu/dist/f/666/files/2018/07/MLA150-7-17-18-2ka85rb.pdfLithography/Photolithography (Resist, Exposure, Develop, Oven/Hotplate)TrainingHeidelberg MLA150PDF / Word Doc
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Soft and Hybrid Nanotechnology Experimental (SHyNE) ResourceMaskless Aligner – Heidelberg uPG501The µPG 501 is a tabletop maskless aligner system (Figure 1). It can be used for direct-writing as well as for making photomaskshttps://cpb-us-e1.wpmucdn.com/sites.northwestern.edu/dist/f/666/files/2015/10/maskless_aligner_10222015-23ndtn9.pdfLithography/Photolithography (Resist, Exposure, Develop, Oven/Hotplate)TrainingHeidelberg uPG501PDF / Word Doc
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Soft and Hybrid Nanotechnology Experimental (SHyNE) ResourceUltraviolet Flood Exposure System – Inpro Technologies F300Shttps://cpb-us-e1.wpmucdn.com/sites.northwestern.edu/dist/f/666/files/2015/10/Ultraviolet_Flood_Exposure_System_Inpro_Technologies_F300S-1flclno.pdfLithography/Photolithography (Resist, Exposure, Develop, Oven/Hotplate)TrainingInpro Technologies F300SPDF / Word Doc
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Soft and Hybrid Nanotechnology Experimental (SHyNE) ResourceVacuum Oven – YEShttps://cpb-us-e1.wpmucdn.com/sites.northwestern.edu/dist/f/666/files/2015/10/Yes5_Manual-12xsf84.pdfLithography/Photolithography (Resist, Exposure, Develop, Oven/Hotplate)TrainingYES 5PDF / Word Doc
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Soft and Hybrid Nanotechnology Experimental (SHyNE) ResourceConvection Ovens – Blue M DCC-146-C-ST350Blue-M ovens are for baking photoresist on silicon or quartz/glass wafers onlyhttps://cpb-us-e1.wpmucdn.com/sites.northwestern.edu/dist/f/666/files/2015/10/ConvectionOvensBlueMDCC_146_C-ST350-1svrt58.pdfLithography/Photolithography (Resist, Exposure, Develop, Oven/Hotplate)TrainingBlue M DCC-146-C-ST350PDF / Word Doc
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nano@stanfordHow to characterize thin ALD filmsBoth electrical and physical characterization techniques are explained for characterizing thin ALD films.https://snfexfab.stanford.edu/snf/nano-nugget/how-to-characterize-thin-ald-filmsMetrology (Ellipsometry, Profilometry, film characterization)Surface Analysis
Training - more specific information focused on a tool and/or processing or recipes for that tool
Intro/BackgroundPDF / Word Doc
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San Diego Nanotechnology Infrastructure (SDNI)Veeco SPMStandard Operating Procedure (SOP) and learning materials for Veeco Scanning Probe Microscope / Atomic Force Microscope (SPM/AFM)-Metrology (Ellipsometry, Profilometry, film characterization)TrainingVeeco SPMPDF / Word Doc
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San Diego Nanotechnology Infrastructure (SDNI)Filmetrics Profilm3D SOPStandard Operating Procedure (SOP) and learning materials for Filmetrics Profilm3D intermetric profiler system-Metrology (Ellipsometry, Profilometry, film characterization)TrainingFilmetrics Profilm3DPDF / Word Doc
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Soft and Hybrid Nanotechnology Experimental (SHyNE) ResourceZygo 3D Optical ProfilerNexview 3D optical surface profiler excels at measuring all surfaces – from supersmooth to very rough, with sub-nanometer precision, independent of field of view. Measurement types include flatness, roughness, large steps and segments, thin films, and steep slopes, with feature heights ranging from < 1 nm up to 20000 µm. https://cpb-us-e1.wpmucdn.com/sites.northwestern.edu/dist/f/666/files/2015/10/3D_Optical_ProfilerZygo-1bcm1fu.pdfMetrology (Ellipsometry, Profilometry, film characterization)TrainingZygo 3D Optical ProfilerPDF / Word Doc
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Soft and Hybrid Nanotechnology Experimental (SHyNE) ResourceContact Angle Measurement – VCA Optima XEThe VCA Optima Contact Angle Measurement system (Figure 1) incorporates lightweight design, easy assembly, and the latest Windows standards and user‐friendly software to create a contact angle instrument that is accurate and easy to use. VCA‐optima is suitable for research or quality control in R&D and process engineering. The system integrates contact angle and surface energy evaluation with computer imaging technology to create an easy to use tool that provides accurate, objective results. https://cpb-us-e1.wpmucdn.com/sites.northwestern.edu/dist/f/666/files/2015/10/Contact_Angle_Measurement_VCAOptima_XE-2fpdf32.pdfMetrology (Ellipsometry, Profilometry, film characterization)TrainingVCA Optima XEPDF / Word Doc
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Soft and Hybrid Nanotechnology Experimental (SHyNE) ResourceReflectometer – Filmetrics F20https://cpb-us-e1.wpmucdn.com/sites.northwestern.edu/dist/f/666/files/2015/10/Reflectometer_Filmetrics_F20-1yihl3t.pdfMetrology (Ellipsometry, Profilometry, film characterization)TrainingFilmetrics F20PDF / Word Doc
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Soft and Hybrid Nanotechnology Experimental (SHyNE) ResourceSpectroscopic Ellipsometer – J.A. Woollam alpha-SEhttps://cpb-us-e1.wpmucdn.com/sites.northwestern.edu/dist/f/666/files/2018/05/Ellipsometer_sop-V2_0405-nb-1966x6j.pdfMetrology (Ellipsometry, Profilometry, film characterization)TrainingJ.A. Woollam alpha-SEPDF / Word Doc
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Soft and Hybrid Nanotechnology Experimental (SHyNE) ResourceStylus Profilometer – Veeco Dektak-8https://cpb-us-e1.wpmucdn.com/sites.northwestern.edu/dist/f/666/files/2015/10/Stylus_Profilometer_Veeco_Dektak-8-1sfjb5o.pdfMetrology (Ellipsometry, Profilometry, film characterization)TrainingVeeco Dektak-8PDF / Word Doc
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nano@stanfordTips- Using Keyence for X-sectional ImagingTips for using the Keyence to image cross sections of wafer pieces. This can be used as a quick check before X-SEM.https://snfexfab.stanford.edu/snf/nano-nugget/tips-using-keyence-for-x-sectional-imagingMicroscopy / Imaging (SEM, TEM, FIB, optical, AFM)TrainingKeyence Digital Microscope VHX-6000PDF / Word Doc
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nano@stanfordCross-sectional Characterization of Transferred DSA Holes using Focus Ion BeamHere, we describe our strategy for inspecting the cross-section of features transferred from the BCP into an underlying hard material (e.g. SiO2, Si).
https://snfexfab.stanford.edu/snf/nano-nugget/cross-sectional-characterization-of-transferred-dsa-holes-using-focus-ion-beam
Microscopy / Imaging (SEM, TEM, FIB, optical, AFM)TrainingHeidelberg MLA 150PDF / Word Doc
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San Diego Nanotechnology Infrastructure (SDNI)FEI Apreo SEM SOPStandard Operating Procedure (SOP) and learning materials for FEI Apreo Scanning Electron Micrscope (SEM)-Microscopy / Imaging (SEM, TEM, FIB, optical, AFM)Metrology (Ellipsometry, Profilometry, film characterization)TrainingFEI ApreoPDF / Word Doc
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San Diego Nanotechnology Infrastructure (SDNI)FEI Quanta SEM SOPStandard Operating Procedure (SOP) and learning materials for FEI Quanta Scanning Electron Micrscope (SEM)-Microscopy / Imaging (SEM, TEM, FIB, optical, AFM)Metrology (Ellipsometry, Profilometry, film characterization)TrainingFEI Quanta FEG 250PDF / Word Doc
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San Diego Nanotechnology Infrastructure (SDNI)Zeiss Sigma SEM SOPStandard Operating Procedure (SOP) and learning materials for Zeiss Sigma Scanning Electron Micrscope (SEM)-Microscopy / Imaging (SEM, TEM, FIB, optical, AFM)Metrology (Ellipsometry, Profilometry, film characterization)TrainingZeiss Sigma 500PDF / Word Doc
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Soft and Hybrid Nanotechnology Experimental (SHyNE) ResourceAtomic Force Microscope – Bruker EdgeThe Dimension Edge Scanning Probe Microscope (SPM) produces high-resolution, three dimensional images by scanning a sharp tip over the sample surface. The tip is part of a flexible cantilever, which extends from a solid substrate. The tip-cantilever-substrate component is driven by piezo tube and controlled by closed loop driving system, to produce atomic level precision images. https://cpb-us-e1.wpmucdn.com/sites.northwestern.edu/dist/f/666/files/2019/07/SOP-AFM.pdfMicroscopy / Imaging (SEM, TEM, FIB, optical, AFM)Surface AnalysisTrainingBruker EdgePDF / Word Doc
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Soft and Hybrid Nanotechnology Experimental (SHyNE) ResourceMicroscope – Nikon LV150This upright optical microscope is designed for investigating up to 150 mm (6 inch) semiconductor wafers but can also be used for fragments and many other types of samples. It can capture colored images and record high-speed videos.https://cpb-us-e1.wpmucdn.com/sites.northwestern.edu/dist/f/666/files/2015/10/Microscope_characterization-03072018-nb-2mes07c.pdfMicroscopy / Imaging (SEM, TEM, FIB, optical, AFM)TrainingNikon LV150PDF / Word Doc
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Soft and Hybrid Nanotechnology Experimental (SHyNE) ResourceJEOL ARM300F GrandARM TEMhttp://www.nuance.northwestern.edu/docs/epic-pdf/JEOL_ARM300F_manual.pdfMicroscopy / Imaging (SEM, TEM, FIB, optical, AFM)Chemical / Composition Analysis (Raman, FTIR, UV/Vis, EDS, EBSD)TrainingJEOL ARM300F GrandARM TEMPDF / Word Doc
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Soft and Hybrid Nanotechnology Experimental (SHyNE) ResourceESEM - Wet SEM Quanta 650FSEM training SOPhttp://www.nuance.northwestern.edu/docs/epic-pdf/2020_user-manuals/esem_3_2020.pdfMicroscopy / Imaging (SEM, TEM, FIB, optical, AFM)Chemical / Composition Analysis (Raman, FTIR, UV/Vis, EDS, EBSD)TrainingFEI Quanta 650FPDF / Word Doc
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Soft and Hybrid Nanotechnology Experimental (SHyNE) ResourceFEI Quanta 650 ESEMhttp://www.nuance.northwestern.edu/docs/epic-pdf/2020_user-manuals/quanta_3_2020.pdfMicroscopy / Imaging (SEM, TEM, FIB, optical, AFM)Chemical / Composition Analysis (Raman, FTIR, UV/Vis, EDS, EBSD)TrainingFEI Quanta 650 ESMPDF / Word Doc
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Soft and Hybrid Nanotechnology Experimental (SHyNE) ResourceHitachi S4800-II cFEGhttp://www.nuance.northwestern.edu/docs/epic-pdf/2020_user-manuals/hitachi_4800_3_2020.pdfMicroscopy / Imaging (SEM, TEM, FIB, optical, AFM)Chemical / Composition Analysis (Raman, FTIR, UV/Vis, EDS, EBSD)TrainingHitachi S4800-II cFEGPDF / Word Doc
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Soft and Hybrid Nanotechnology Experimental (SHyNE) ResourceHitachi S-3400N-II SEMhttp://www.nuance.northwestern.edu/docs/epic-pdf/2020_user-manuals/3400n_3_2020.pdfMicroscopy / Imaging (SEM, TEM, FIB, optical, AFM)Chemical / Composition Analysis (Raman, FTIR, UV/Vis, EDS, EBSD)TrainingHitachi S-3400N-IIPDF / Word Doc
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Soft and Hybrid Nanotechnology Experimental (SHyNE) ResourceHitachi SU-8030 FEG SEMhttp://www.nuance.northwestern.edu/docs/epic-pdf/2020_user-manuals/hitachi_8030_3_2020.pdfMicroscopy / Imaging (SEM, TEM, FIB, optical, AFM)Chemical / Composition Analysis (Raman, FTIR, UV/Vis, EDS, EBSD)TrainingHitachi SU-8030PDF / Word Doc
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Soft and Hybrid Nanotechnology Experimental (SHyNE) ResourceJEOL 7900FLV SEMhttp://www.nuance.northwestern.edu/docs/epic-pdf/2020_user-manuals/7900_3_2020.pdfMicroscopy / Imaging (SEM, TEM, FIB, optical, AFM)Chemical / Composition Analysis (Raman, FTIR, UV/Vis, EDS, EBSD)TrainingJEOL 7900FLVPDF / Word Doc
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Soft and Hybrid Nanotechnology Experimental (SHyNE) ResourceHitachi HD-2300A STEMhttp://www.nuance.northwestern.edu/docs/epic-pdf/HD2300_Daily_Operation_Guide_v6.pdfMicroscopy / Imaging (SEM, TEM, FIB, optical, AFM)Chemical / Composition Analysis (Raman, FTIR, UV/Vis, EDS, EBSD)TrainingHitachi HD-2300APDF / Word Doc
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Soft and Hybrid Nanotechnology Experimental (SHyNE) ResourceJEOL JEM-2100F TEMhttp://www.nuance.northwestern.edu/docs/epic-pdf/JEOL_2100F_manual_2017.pdfMicroscopy / Imaging (SEM, TEM, FIB, optical, AFM)Chemical / Composition Analysis (Raman, FTIR, UV/Vis, EDS, EBSD)TrainingJEOL JEM-2100FPDF / Word Doc
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nano@stanfordCharacterization of TMDs and Contact schemes for Photovoltaic Applications- Standard Operating ProcedureThe standard operating procedures for 1. Optimal TMD exfoliation on SiO2 substrate, 2. Etching of TMD flakes, 3. Transfer from TMD flakes from SiO2 substrate to a metallic substrate are explained in details.
https://snfexfab.stanford.edu/snf/nano-nugget/characterization-of-tmds-and-contact-schemes-for-photovoltaic-applications-standard-operating
Miscellaneous TrainingPDF / Word Doc
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nano@stanfordAu-Sn Eutectic chip-bonding for high heat flux vapor chamber applications using Flip Chip Bonder: Suggestions and TipsHere are some getting started tips for use of Pyrex wafers in the SNF lithography and Flip Chip Bonding equipment.
https://snfexfab.stanford.edu/snf/nano-nugget/au-sn-eutectic-chip-bonding-for-high-heat-flux-vapor-chamber-applications-using-flip-chip-bonder
Miscellaneous TrainingFinetech LambdaPDF / Word Doc
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nano@stanfordWhite Paper: Introduction to the Green Gap Project: InGaN-GaN Multiple Quantum Wells for Green LEDs on SiThis phenomenon is known as ‘green gap’. This document provides a brief background into the technical challenges that inspired the Green Gap E241 project.https://snfexfab.stanford.edu/snf/nano-nugget/white-paper-introduction-to-green-gap-project-ingan-gan-multiple-quantum-wells-for-green-leds-on-siMiscellaneous TrainingAix-ccsPDF / Word Doc
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nano@stanfordFinetech Lambda Flipchip Bonder and Process Integration New User Tips“Tips” or “tricks” on use of the Lambda Flipchip Bonder and the integration with lithography and metallization steps that are used in preparation for bonding.https://snfexfab.stanford.edu/snf/nano-nugget/finetech-lambda-flipchip-bonder-and-process-integration-new-user-tipsMiscellaneous Intro/BackgroundFinetech LambdaPDF / Word Doc
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San Diego Nanotechnology Infrastructure (SDNI)UCSD Nano3 Facility Online Manager (FOM)SOPs for most instrumentation; accessible to users via their user accounts; the SOPs are very instrument specific.https://nano3fom.eng.ucsd.edu/fom/Miscellaneous TrainingPDF / Word DocUnlicensed
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San Diego Nanotechnology Infrastructure (SDNI)Minitech Micromill CNCStandard Operating Procedure (SOP) and learning materials (fusion 360 software quick start) for Minitech micromill CNC-Miscellaneous SoftwareTrainingMinitech Micromill CNCPDF / Word Doc
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Soft and Hybrid Nanotechnology Experimental (SHyNE) ResourceVacuum Atmospheres Company OMNI-LAB Glovebox Systemhttp://www.vac-atm.com/pdf/tb1965v2-5.pdfMiscellaneous Training
Vacuum Atmospheres Company OMNI-LAB
PDF / Word Doc
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Soft and Hybrid Nanotechnology Experimental (SHyNE) ResourceBall Wire Bonder – iBond5000The iBond 5000 is a ball bonder for making electrical interconnections between a chip and the package. Ball bonding processes use a combination of heat, pressure, and ultrasonic energy to make a weld at each end of the wire.https://cpb-us-e1.wpmucdn.com/sites.northwestern.edu/dist/f/666/files/2016/02/Wire-bonder-16bjnmx.pdfMiscellaneous TrainingiBond5000PDF / Word Doc
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Soft and Hybrid Nanotechnology Experimental (SHyNE) ResourceLaser Cutter – LPKF ProtoLaser RLPKF Protolaser R is a full-scale production level CNC laser cutter which can be used to cut or ablate materials such as PCBs, Si wafers, glass, metals and polymers such as PDMS and Polyimide. https://cpb-us-e1.wpmucdn.com/sites.northwestern.edu/dist/f/666/files/2015/10/ProtoLaser-R_SOP_v2-rh7ic3.pdfMiscellaneous Training LPKF ProtoLaser RPDF / Word Doc
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Soft and Hybrid Nanotechnology Experimental (SHyNE) ResourceWedge Bonder – West Bond 747677Ehttps://cpb-us-e1.wpmucdn.com/sites.northwestern.edu/dist/f/666/files/2018/05/Wedge-bonder-training-manual_03132018-1qm7owc.pdfMiscellaneous TrainingWest Bond 747677EPDF / Word Doc
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Soft and Hybrid Nanotechnology Experimental (SHyNE) ResourceElectrical Test StationThe electrical test probe station is for semiconductor device characterization and analysis at ambient environment. The Agilent 4155C semiconductor parameter analyzer (SPA) has standard test routines for p-n junctions, CMOS, MOSFET, diodes etc. The Agilent 4285A LCR meter is for CV measurements of dielectric materials and capacitors. https://cpb-us-e1.wpmucdn.com/sites.northwestern.edu/dist/f/666/files/2015/10/Electrical-Test-Station-126ni13.pdfMiscellaneous TrainingAgilent 4155C semiconductor parameter analyzer (SPA), Agilent 4285A LCR meterPDF / Word Doc
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Texas Nanofabrication Facility (TNF)Graduate Portfolio Program in NanomanufacturingNanomanufacturing Portfolio Programhttps://utexas.app.box.com/s/yi7i4q2ovsq2w9qco3ij5jomghmv1i11Miscellaneous MiscCourse descriptionPDF / Word Doc0Copyrighted
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Soft and Hybrid Nanotechnology Experimental (SHyNE) ResourceFurnaces – TystarTystar #1 Wet/Dry Oxidation Furnace, Tystar #2 Atmospheric Anneal Furnace Tystar #6 LPCVD, Low- stress Nitride Furnacehttps://cpb-us-e1.wpmucdn.com/sites.northwestern.edu/dist/f/666/files/2015/10/Furnace_Tystar-1hj2q7h.pdfOxidation and AnnealingTrainingTystar multiplePDF / Word Doc