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Annexure-IV
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Technical Specifications of ICP-OES
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ICP-OES for simultaneous multi-elemental analysis at higher concentration and trace levels along with spray chamber, sample introduction system, RF generator and auto sampler. Instrument should meet the global food regulation requirements (like CODEX, USFDA, EU, FSSAI, etc.). The ICP-OES system should be able to determine all major and trace elements in a single method.COMMENTS JUSTIFICATION
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SI. No.Instrument ComponentRequired Specifications
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1Technology(i) System must be Simultaneous polychromator based dual view ICP-OES Spectrometer. Dual view (Axial & radial) along with rapid/fast switching.
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(ii) The instrument must include appropriate ICP torch and Concentric Quartz nebulizer (Acid Resistive) spray chamber system.
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2Peristatic Pump (i) 3 or more channel. Pump speed with 70 rpm or better
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3RF Generator(i) Should have software-controlled RF generator with frequency of 25-50 MHz. The RF must be variable & adjustable from 750 to 1500 watts or wider along with suitable increment step
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4Software controlled Flow Controller with ≤1 L/min increments(i) Three Nos. or more variable & software-controlled gas flow controllers (MFC/EFC) with ≤ 1 L/min or lower increment step for precise control of Plasma, Nebulizer, Aux & makeup/additional gas for gas.
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(ii)  The instrument must monitor all gas pressure through mass flow control or electronic flow control.
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(iii)  Plasma ignition and shut down must be computer controlled and totally automated.
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(iv) All gas requirements for plasma gas, nebulizer gas, auxiliary gas, purge gas, & sheer gas must be clearly mentioned.
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5Auto Sampler(i) System should be equipped with auto sampler with minimum 180 samples positions or more.
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(ii) The autosampler should have LED status light for real-time operating status.
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(iii) The autosampler should have movement in three axes (X-Y-Z) to acceleration and deceleration speed.
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(iv) System should include all accessories, racks, bottles, tubing, water container, etc.
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6Optics(i) Must have Echelle-based polychromator.
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(ii)   Resolution: 7pm @ 200/202 nm or better.
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(iii) Radial viewing height automatic adjustment should be upto 18mm or more.
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7Detector(i) The system should be a true  simultaneous with two detector system or synchronous technology with CCD detector system or charge injection device detector system.
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(ii) CID or CCD or SCD with Integration/readout time must be ≤ 15 sec.
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(iii) Wavelength range: of 165–750nm or suitable range to cover elements as per ICP OES technology.
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(iv) Peltier device with cooling at -30 Deg C or Below for reducing or optimizing Dark current /Photometric Noise.
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(v) The actual resolution (not the pixel resolution) of the system should be ≤ 0.009 nm at 200nm.
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(vi)The spectrometer must cover full spectral range from 165-750 nm or better with capability of measuring UV wavelengths without any compromise on sensitivity.
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(vii) The resolution of the system must be 0.007nm or less at around 200nm.
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(viii) The entire optical system must be closed in an argon/nitrogen purged and thermo stated optical enclosure.
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(ix) Viewing of the plasma must be computer controlled (Dual View).
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(x) The system should have option of selecting any wavelength in any mode (axial/radial).
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(xi) The instrument must be able to perform determinations across the entire spectrum, both UV and Visible 165 - 750 nm
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8Software(i)  Latest licensed software to control all the modules of ICP-OES.
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(ii) Software update should be provided free of cost, upto minimum 10 Years.
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(iii) Instrument control, acquire, store, process and reproduce the data, report generation, self-diagnosis and auto-tuning.
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(iv) Auto Start-up and shutdown of the instrument or it should be possible using a single key operation.
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(v) Software must be 21 CFR part 11 compliant and minimum 2 offline licences must be offered as a standard supply.
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(vi) Compatible with windows 10 or latest version
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(vii) Software should also have comprehensive wavelength library with indication of preferred line for each element.
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(viii)It should feature automatic identification of possible spectral interferences when selecting wave lengths for analysis and should have search mode for identification of unknown wave lengths.
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9Standard Items(i)  Exhaust hood for ICP-OES & autosampler.
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(ii) 20 KVA online UPS with 60 min backup along with 02 MCB (in & Out) & 80 meter cable
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(iii) Six (06) Argon cylinders with 02 stage brass double stage regulator & four stage Manifold.
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(iv) Reputed Brand chiller for instrument.
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(v)    Gas panel & exhaust Hood for ICP-OES and Autosampler.
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(vi) Factory fitted Branded i7 PC ,1TB SDD,32 GB RAM, 21 inch Monitor, Color Laser multifunctional duplex Printer & MS office.
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(vii) Reputed brand, diretly from the OEM supplied, scroll noise & oil free Air compressor (if required)
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(viii) Multielement Aqueous Standards (21-22 Elements) of 250 ml of 1000 ppm, traceable to ISO 17034
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(ix) Single element standards (including Arsenic, Mercury & Selenium) of 100 ml of 100ppm) traceable to ISO 17034.
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 (x) Wavelength calibration solution 500ml, 5ppm (13-14 element mix) : Qty - 021 Nos
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(xi)  Internal mix standard aqueous (traceable to ISO 17034) :- 125ml
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(xii)  Calibration blank solution ASTM Type 1 Water (500ml) : Qty -02 No
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(xiii) Latest version of 21 CFR Compliance Software must be provided with the system.
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(xiv) ICPOES /ICPMS grade suprapure Acids for trace analysis: Nitric acid (HNO3) & Hydrochloric acid (HCL) - 15 L each.
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(xv) 02 Nos PP waste container (15 L each)
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10Standard Accessories (i) 180 Vial or more position Autosampler with enclosers & to remove toxic fumes. 1200 vial for Autosampler should be included.
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(ii) Semi volatile organic dedicated kit for edible oil analysis. Along with nebulizer, torch, injector spray chamber, tubings, oxygen variable MFC, Organics standard 21 element mix/single element standard (100gm), internal standard (100 gm), solvent for mixing /makeup (3L), all standards traceable to ISO 17034
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(iii) Internal standard kit
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(iv) Hydride generating accessories kit along with Separate & dedicated spray chamber & tubing set (Reductant & Waste -pk/12 each) should be offered for low ppb As, Se, Sn & Hg.
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11Consumables
(Must be quoted with OEM P/N.)		(i) Standard Peristatic Pump Tubing set for sample intake Pk/12 (04 Set each)
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(ii) Standard Peristatic Pump Tubing set for rinse /Drainage: Pk/12 (04 Set each)
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(iii) Standard Peristatic Pump Tubing set for Internal standard . Pk/12 (04 Set each)
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(iv) Organic solvent Tubing set for sample intake Pk/12 (04 Set each)
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(v) Organic solvent Peristatic Pump Tubing set for rinse /Drainage: Pk/12 (04 Set each)
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(vi)  Standard spray chamber (01 Nos)
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(vii) Standard Nebulizer -02 Set.
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(viii) Standard Torch & injector: (02 Set)
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(ix) Standard Spray chamber drain tubing (02 each)
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(x) Autosampler tubing set Pk/12 (02 set)
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(xi) Nebulizer capillary tubing - 01 Meter (04 Set)
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(xii) PFA tubing for gas supplies to nebulizer- 1 Meter- (03 Set)
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(xiii) Drain tubing for spray chamber waste -03 Sets
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(xiv) Hydride kit peristatic pump tubing for reductant & Waste -pk/12 (02 sets each)
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(xv) Autosampler vessel -1000 Nos
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12Warranty & IQ/OQ/PQ(i)   Five year warranty included local/third party items i.e. ICP-OES, Chiller, UPS, PC, Microwave Digestion System, Printer, exhaust, regulators, Exhaust etc (excluding consumables items) IQOQ for hardware & CFR software must be offered with system.
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(ii)  Per year Operational Qualification (OQ) per Year 2nd to 5th Year.
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(iii) Per Year two PM visit with comprehensive PM Kit for ICP-OES and Microwave Digestion System. ICP-OES PM kit must include Radial & Axial Pre-Optic Window, chiller fluid, ICPOES purge gas instrument filter, Air inlet filter elements ,connector tubing’s etc. OEM Document for Scope of comprehensive PM kit must be enclosed.
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(iv) On site IQ, OQ of instrument along with document to be provided
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(v) Supplier to assist till satisfactory PQ of instrument
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 (vi) It should cover hardware, software as well as wear and tear consumables (except column and sample preparation), Up-gradation of software to the latest version (if applicable), prompt service (within 24 hours on-call), training and application support during the period.
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(vii) In case of breakdown of the system, the query has to be attended immediately within 24 hrs & servicing to be done within 48 hrs by the supplier during the warranty period and incase of major breakdown, maximum down time period is 1 Week, if it’s not attended the warranty will extend accordingly.
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13After sales service/ Post warranty(i) Should have a good after sales service/technical support capable of reaching at short notice the places where ICP-OES is proposed to be installed. Visits and unlimited breakdown calls by service/application support, engineers should attend immediately without fail for ICP-OES including Chiller and UPS system.
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(ii) Troubleshooting training (Instrumentation/Application) as and when required free of cost.
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(iii) The vendor should also assure supply of spares, accessories, consumables and service for at least 10 years.
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(iv) Comprehensive AMC cost/rate for ICP-OES including Chiller to be quoted separately. Terms and conditions for the comprehensive AMC after the warranty period has to be specified. AMC/CMC price quoted by the vendor will be considered as independent price. It will not be considered for finalizing the L1.
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14After sales service/ Post warranty(i) Should have a good after sales service/technical support capable of reaching at short notice the places where ICP-OES is proposed to be installed. Visits and unlimited breakdown calls by service/application support, engineers should attend immediately without fail for ICP-OES including Chiller and UPS system.
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(ii) Troubleshooting training (Instrumentation/Application) as and when required free of cost.
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(iii) The vendor should also assure supply of spares, accessories, consumables and service for at least 10 years.
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(iv) Comprehensive AMC cost/rate for ICP-OES including Chiller to be quoted separately. Terms and conditions for the comprehensive AMC after the warranty period has to be specified. AMC/CMC price quoted by the vendor will be considered as independent price. It will not be considered for finalizing the L1.
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15Compliance Statement (i) All the technical specifications given in the tender document must be supported by printed leaflets / brochures and must comply the working performance of the equipment at the time of installation and demonstration
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(ii)The quote should also include a compliance statement vis-à- vis, specifications in a “tabular form” clearly stating the compliance and giving justification, if any supported by technical literature.
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(iii) This statement must be signed, with the company seal, for its authenticity and acceptance that any incorrect or ambiguous information found submitted will result in disqualification.
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16PrinterLaserJet Printer – B/W with LAN, Network Card and Bluetooth facility.
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17Installation & application training(i) Vendor must include installation and Training at user site. Apart of installation, Application training for 5 days every year ( for 02 personells per installation site) at their application center by certified application engineer including all boarding / lodging & transportation .
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18Experience: (i) The supplier should have executed at least Minimum 20 or more of the model/series of model quoted successful installations among which 5 should be installed in Government institutes.
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(ii) The Complete users list for the quoted model in India, with contact addresses, emails and phone numbers should be provided.
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Microwave Digestion System
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RequirementSpecification
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19General(i) The instrument should have a superior pressure venting which is not temperature dependent so as to prevent any loss of volatile metals and should have homogeneous microwave field to avoid sample burning
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20System(i) Microwave digestion system should have temperature and pressure control mechanism.
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(ii) The system should be software controlled.
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(iii) Necessary consumables and maintenance parts should also be quoted to run instrument trouble free