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The Arizona STEM Acceleration Project

Mystery Powders

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Crime Busters: Mystery Powders

A 5th Grade STEM Lesson

Author: Tonya Page

Date: Jan 3, 2023

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Notes for Teachers

Prior to the lesson: (30 min)

  • Students should have a strong understanding of data collection and representation through qualitative and quantitative observations.
  • Students will complete a reading, video and assessment on physical and chemical changes that may occur when substances are mixed.
  • Students should have all safety and lab protocols safely in place.

During the lesson:

  • This lesson takes place in one 60 minute session.
  • Students may work in groups of 2-4 to test to identify unknown powders. They must wear protective goggles and follow all safety procedures which you should establish beforehand.
  • An emphasis on collecting quantitative and qualitative data through observations of interactions between materials.

List of Materials

  • Mystery Powders: (1 tbsp for each group)
    • salt
    • granulated sugar
    • flour
    • cornstarch
    • baking soda�
  • Liquids to test:
    • vinegar
    • water
    • iodine solution
  • Supplies:
    • mL dropper for each liquid
    • spoon
    • magnifying glass
    • wax paper
    • protective goggles
    • scale
    • correlating worksheets

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Science & Math Standards

Arizona Science Standards

5.P1U1.2 Plan and carry out investigations to demonstrate that

some substances combine to form new substances with

different properties and others can be mixed without

taking on new properties.

Next Generation Science Standards

5-PS1-2. Measure and graph quantities to provide evidence that regardless of the type of change that occurs when heating, cooling, or mixing substances, the total weight of matter is conserved.

5-PS1-3. Make observations and measurements to identify materials based on their properties.

5-PS1-4.Conduct an investigation to determine whether the mixing of two or more substances results in new substances.

Math Standards:

5.MD.A.1 Convert among different-sized standard measurement units within a given measurement system, and use these conversions in solving multi-step, real-world problems.

5.G.A.2 Represent real-world and mathematical problems by graphing points in the first quadrant of the coordinate plane, and interpret coordinate values of points in the context of the situation.

ELA Standards

5.RI.1 Quote accurately from a text when explaining what the text says explicitly and when drawing inferences from the text.

5.RF.4 Read with sufficient accuracy and fluency to support comprehension.

5.W.2 Write informative/explanatory texts to examine a topic and convey ideas and information clearly.

5.W.1 Write opinion pieces on topics or texts, supporting a point of view with reasons and information.

5.W.4 Produce clear and coherent writing in which the development and organization are appropriate to task, purpose, and audience.

5.W.6 With some guidance and support from adults, use technology, including the internet, to produce and publish writing as well as to interact and collaborate with others; demonstrate sufficient command of keyboarding skills in order to complete a writing task.

5.W.7 5.W.8 Conduct short research projects that use several sources to build knowledge through investigation of different aspects of a specific question or topic.

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Objective(s):

Today students will collaborate and communicate together to solve a problem through inquiry and investigation while using qualitative and quantitative observations to identify multiple mystery powders and their characteristics of physical and chemical reactions when mixed with known substances.

Today students will compare and contrast observations of pertinent details taken while investigating.

Today students collaborate to collect qualitative and quantitative measurements to identify unknown cupboard ingredients.

Today students will use science and engineering practices to effectively problem solve.

Today students will effectively communicate their data and inquiry results.

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Agenda (90 minutes)

Pre Teach (30 min)

What are qualitative and quantitative observations?

What are physical and chemical changes?

How can I practice safety throughout lab experiments?

Lesson (60 min)

Introduction to Forensics careers

A day in the life of a forensics technician

A day in the forensics lab

CSI: Introduction to the crime- Who stole it?

Forensics video-how to test unknown powders

Distribute materials and guidelines

Experimentation time/Hands-on Activity

Share or Present findings

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Pre-teach

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Qualitative observations are those that describe the situation using anything that does not use a number or measure. For example, the sun is bright today.

Qualitative Examples:

gender

religion or marital status

color

native language

social class

bubbles

heat

sizzling

steam

method of treatment

Quantitative observations are those that use a number in the description (weight, time, number of items, height, volume, and so on). For example, the temperature is 78 degrees Fahrenheit right now.

Quantitative Examples

age

height

weight

income

group size

test scores

shoe size

percentages

ratings

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In a physical change, the material involved in the change is structurally the same before and after the change. Types of some physical changes are texture, shape, temperature, and a change in the state of matter. A change in the texture of a substance is a change in the way it feels. For instance, a block of wood may feel rough when you run your finger across it but rubbing the wood with sandpaper smooths the surface so it no longer feels rough. The wood itself has not changed during sanding to become a new material, only the texture of the surface changed. A piece of metal may be heated in a fire until it glows, but the metal is the same material before heating and after cooling. Similarly, when a material changes phase, it only changes physically; the substance is still the same. Think about ice melting into water, and then water being heated up and turning into steam. The chemical structure of water is the same whether it is a solid (ice), liquid, or gas (steam).

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What is a Chemical Change?

A chemical change occurs when the composition of a substance is changed, which requires the breaking and forming of chemical bonds during a chemical reaction. This results in the rearranging of atoms in substances to form the products of a chemical reaction, which are brand new molecules that cannot be easily reverted back to their original state.

Sometimes it is difficult to tell if a chemical reaction has taken place. To help determine whether there has been a reaction, chemists consider the basic indicators that a reaction has occurred, such as a change in temperature, a change in color, the development of an odor, the formation of a precipitate, or the formation of a gas.

In a chemical alteration, the temperature change occurs as a result of the breaking or formation of chemical bonds. When the chemical bonds of the reactants are broken, sometimes excess energy is released, causing heat to be discharged, and leading to an increase in temperature. Alternatively, a reaction may require energy from the environment in order to take place, causing heat to be absorbed, and leading to a decrease in temperature. Burning wood is an example of a reaction that releases excess energy as heat. A chemical cold pack in a first aid kit is an example of a chemical reaction that absorbs heat energy resulting in cooling.

An example of a color change signaling a chemical reaction can be observed when iron reacts with oxygen to produce iron oxide, such as when an iron nail is left outside, and it develops a reddish-brown rust.

Rotting food is an example of odor development as a result of a chemical change. When food is left out for too long, or it reaches its expiration date, it eventually spoils, often producing a foul odor in its rotten state. This is because of chemical reactions that take place as the food begins to break down and go bad, which leads to the formation of new substances that have unique smells associated with them.

Another common sign of a chemical reaction is the formation of a precipitate. This happens when chemicals dissolved in a solution are mixed together and an insoluble solid, known as a precipitate, forms in the liquid mixture. The creation of a new, solid substance from two liquid substances indicates that a reaction has taken place and altered the original substances.

A common chemical reaction is the mixing of vinegar and baking soda. When these two household chemicals are mixed together, it immediately starts bubbling and foaming. The bubbles are a release of carbon dioxide gas, a product of the chemical reaction between the baking soda and vinegar.

Remember that the difference between a physical reaction and chemical reaction is that a chemical reaction cannot be easily reversed, if at all.

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Mystery Powders Lesson

How can you use forensics science techniques with qualitative and quantitative data observations to help solve crimes in the real world?

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Instructions

In groups of 2-4 use forensics science experiment techniques to match known chemical reactions of unknown powders to find a match to the crime scene.

Constraints:

  • 30 minutes
  • Mystery powders: salt, corn starch, powdered sugar, granulated sugar, baking soda
  • Testing liquids: water, vinegar, iodine, cabbage water (optional extension)
  • Tools: mL dropper for each liquid, wax paper
  • Scale to weigh powders to compare

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Notes for Teacher

  • Students will be conducting experiments on 5 unknown substances by dropping different liquids on each of them and collecting data as quantitative and qualitative observations are made.
  • Each group should be given 5 mystery powders (salt, powder sugar, granulated sugar, baking soda, cornstarch) in small bowls. These should be marked only for the teacher to know.
  • Teacher should set aside one “crime” evidence powder to test against the others when establishing which powder they found at the scene of the crime.
  • Correlating worksheets: lab task 1, lab task 2, lab task 3
  • Task 3 is a cheat sheet that will give clues how some substances interact and what to look for. You may want to go over this first.
  • Use wax paper to go under the experiment lab worksheets in order to help keep the mess contained.
  • You may also choose to keep your student’s experiment papers in clear protective sheets or on cooking sheets.

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Hands-on Activity

Lab 1: Distribute the 5 powders for each group. A small sample (1 tsp) should be placed in each circle using a spoon. Students should make and record observations through sight, smell and touch. DO NOT TASTE! The first circle on each row is a control group. No liquid should be dropped on the control group.

Record observations on worksheet: Lab 1.

What does it look like?

What does it smell like?

What does it feel like?

Lab 2: Distribute liquids to test (water, vinegar, iodine) along with mL dropper for each liquid. Use a mL dropper to add 3-5 drops of liquid on each powder and observe changes and reactions. Take notes on chemical and physical properties happening. Students should look for color change, sounds, bubbles, texture differences, etc. See: Chemical and Physical Changes slides.

Lab 3: This may be used as a cheat sheet that will give clues how some substances interact and what to look for. You may want to go over this first for learners who need extra assistance, or use to compare and discuss after.

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Success Criteria

  • Students will be assessed on their ability to make qualitative and quantitative observations of chemical and physical changes in order to correctly match and identify a mystery substance powder.
  • Students will be able to accurately document and analyze their data found through observation in the form of a visual graph or table.
  • Students will be able to identify physical or chemical changes that occur when substances are mixed.
  • Students will use science and engineering practices to inquire, collaborate and obtain, evaluate and communicate information or data found.
  • Students will participate in a class discussion and reflection on their findings.

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Differentiation

  • Lower the number of powders to three instead of five.
  • Go over Lab #3 first to show what physical and chemical properties and changes to look for while mixing the substances.
  • Include data collection and graph making in pre-teaching.
  • Make a graph as a class of observations. (How long did it bubble? Rate the color change 1-5, How much dissolved? etc.)

Remediation

Extension/Enrichment

  • Use additional mystery powders: plaster of paris, powdered sugar, etc.
  • Use cabbage water as an additional liquid to test against. (Materials: purple cabbage, knife, hot water, bowl)
    • Video: Testing with cabbage water
  • For mature students bleach can be used as an alternate liquid.- Bleach should only to be handled by the teacher.
  • Take the investigation further with Chromatography. Write a ransom note for the crime scene. Students will use the science of chromatography to match the pen that was used against 3-4 different types of pens with the same color ink.
  • Video: Ink Chromatography: DIY Crime Scene Invesigators