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How to keep a GREAT natural products notebook

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  • Number 1, most important rule: Do what is sustainable. Consistency is always better than best practices.

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Table of contents

  • Give a general name first such as a project or common traceable thing
  • Then give specifics
  • Don’t forget dates – even every fifth entry or even annual dates are helpful

  • Color codes are helpful (make sure you have enough colors!)

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HPLC

  • Always include gradient either in the chromatogram as separate graph. With time you can refer to same method or name
  • Generally good idea to include UV profile

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Semiprep separation

  • Multiple chromatograms (within reason)
    • Did the collection shift over time?
    • Did the final collection not show certain peaks?
  • Vial weights for only one set of vials
  • Connect fraction to notebook number/vial
  • Run a blank as the last run and be sure to collect. You never know what has accumulated on the column.
  • Suggestion: Give the mass the day you run the vial and prepare the concentration – was it 20, 25, 50 mg/mL? You will have that right here

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Semiprep Separation

  • Alternative views
    • Either multiple runs overlayed
    • Zoom in of certain regions

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Molecular Biology

  • When receiving primers or plasmids it is important to track every step of the process – did you rehydrate? What concentration? What water? Into what container? Where are aliquots being stored?
  • In this example you can see these primers were for checking a synthetic biology target and you can see every step with a two sentence entry from September to October

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Sample Storage