Inst Equip 8.1 - FTIR Cary630

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Quiz for module Inst Equip 8.1 - FTIR Cary630 (IE_8.1_v1)

Name *

zID *

Module Document Declaration

This module is based on the following documents which you must have read, and declared as read, and the following videos which you must declare as viewed:

SCI-CHEMSCI-RMF-7683 - The use of the Agilent Cary 630 FTIR spectrometer
SCI-CHEMSCI-SWP-5429 - The use of the Agilent Cary 630 FTIR spectrometer
Vid-Train-FTIR Cary630-3 - FTIR Cary630 Training Video

PLEASE NOTE:
-> The declaration statement has no bearing on your quiz score.
-> If you have declared the documents as read during a previous quiz attempt, you do not need to declare them as read again.
-> If you have passed the quiz previously but not declared the documents as read, you may declare them as read at any time but you do not need to pass the quiz again.

I declare...

… that I have read the following required documents, and viewed the following required videos (if applicable) for this module and will comply with the instructions and procedures contained within them. (Select all that apply)

SCI-CHEMSCI-RMF-7683

SCI-CHEMSCI-SWP-5429

Vid-Train-FTIR Cary630-3

Module Quiz

1. What sort of samples can you analyse on the FTIR? *

Solids

Liquids

Both

2. How far do you need to turn the sample press knob for a solid sample? *

Until the sample press tip is just 1 cm above your sample

Until you hear the “click” sound

You don’t need to lower it for a solid sample

Until the sample press tip just touches the sample

3. Do you need to close the clamp for a liquid sample? *

Yes

4. How much sample (solid or liquid) is needed for analysis? *

Just enough to cover the diamond sampling window

Enough to cover the stainless-steel circle

5. Prior to every measurement, it is important to clean the crystal and to perform a visual inspection of the diamond sampling window. This is to ensure: *

An accurate background spectrum is collected

An accurate sample spectrum is collected

All the ethanol used to clean the diamond has evaporated

All of the above

6. The user needs to clean the crystal before and after analysis, how will it be done? *

With detergent and kimwipes

Few drops of ethanol and kimwipes

Tissue paper only

Glass pipette

7. What software does the user need to use for analysis of the sample? *

Optimelt

Resolutions – Pro

Cary 630

Win - Pro

8. If the user needs to adjust the gain, what steps do they need to take? *

Advanced features – system check

Advanced features – library management

Advanced features – user management

Advanced features – diagnostics

9. What steps will you take to shut down the instrument? *

Turn off the instrument (clicking on the button)

Close the software on the computer

Log out of ACLS

Shut down the computer

All the above

10. Who do you contact in case of an issue with the instrument? *

Laboratory Manager

Technical Officer

School Manager

PhD supervisor

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